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Growth of Binary Organic Nlo Crystals: M.Na-P.Na and M.Na-CNA System

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Growth of Binary Organic Nlo Crystals: M.Na-P.Na and M.Na-CNA System

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Editor's Note:
Experiments were carried out to grow 3.Nitroaniline (m.NA) crystals doped with 4.Nitroaniline (p.NA) and 2.chloro 4.Nitroaniline (CNA). The measured undercooling for m.NA, p.NA, and CNA were 0.21 tm K, 0.23 tm K, and 0.35 tm K respectively, where tm represents the melting temperature of the pure component. Because of the crystals' large heat of fusion and large undercooling, it was not possible to grow good quality crystals with low thermal gradients. In the conventional two-zone Bridgman furnace we had to raise the temperature of the hot zone above the decomposition temperature of CNA, p.NA, and m.NA to achieve the desired thermal gradient. To avoid decomposition, we used an unconventional Bridgman furnace. Two immiscible liquids, silicone oil and ethylene glycol, were used to build a special two-zone Bridgman furnace. A temperature gradient of 18 K/cm was achieved without exceeding the decomposition temperature of the crystal. The binary crystals, m.NA-p.NA and m.NA-CNA, were grown in centimeter size in this furnace. X-ray and optical characterization showed good optical quality. Singh, N. B. and Henningsen, T. and Hopkins, R. H. and Mazelsky, R. Marshall Space Flight Center NASA ORDER H-20124; F33615-88-C-5506; DCN2-3-10-34841...

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Length 26 Pages
Imprint Createspace Independent Publishing Platform
Released N/A
Identifier (ISBN) 41665580
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National Aeronautics and Space Administration writes contemporary fiction and has always been fascinated by character-driven stories. They hold a degree in English Literature and previously worked as an editor before transitioning to writing their own books. National Aeronautics and Space Administration lives with their spouse and a very vocal rescue cat.

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Jennifer Nelson
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"A highly sophisticated read. The middle had a deliberate pace, but the climax was phenomenal. A solid 4 stars from me."
Sarah Thomas
Sarah Thomas September 09, 2024
"Absolutely brilliant. I became deeply invested in the protagonist's journey. A masterclass in storytelling. A true literary gem."
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Linda Nelson
Linda Nelson December 13, 2025
"Exceeded all my expectations. I became deeply invested in the protagonist's journey. A masterclass in storytelling. An effortless 5 stars."
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"Such a rich narrative. The author orchestrated a breathtaking finale. Truly a work of art. I will undoubtedly revisit this masterpiece."
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